Non-evaporative solid phase ammonium sulfate separation …
Extra pure grade ammonium sulfate ((NH 4) 2 SO 4) (99 %), ammonium hydroxide (NH 4 OH), and sulfuric acid (95%) were purchased from Daejung Chemicals & Metals (Siheung, Korea). Ammonium sulfate reagent was utilized to make a synthetic ammonia-stripped sulfuric acid solution. The 14 water-miscible organic solvents were …
Polyacrylamide Gel Electrophoresis (PAGE): Principle and …
The most commonly used polyacrylamide gel electrophoresis for quantitative protein analysis is Sodium dodecyl sulfate-polyacrylamide gel electrophoresis (SDS-PAGE). ... (%C). Deferring these two parameters, helps in regulation in the pore size of the gel to yield the best separation result. %T indicates the pore size of the prepared gel ...
Recovery of Acid and Base from Sodium Sulfate Containing …
2.1. Materials. We used self-made simulated sodium sulfate waste salt (0.3 mol·L −1) containing lithium carbonate; its components are shown in Table 1 [].H 2 SO 4, NaOH, NaCO 3, and other chemicals used in this study were all analytically pure (Meifeng Chemical Instrument Co. Ltd., Hefei, China).The anion exchange, cation exchange, and …
US3607141A
Process for the recovery and for the separation of pure sodium sulfate and pure ammonium sulfate from aqueous solutions thereof Download PDF Info Publication number US3607141A.
40 Tech News PROVEN METHODS
the solid-liquid separation of the leaching system can become a bottleneck. The ARC process is generally more suitable for larger chloride and potassium removal needs. Evaporated crystals are also pre-dominantly pure sodium sulfate (Figure 5), so the recovery and removal effi ciencies are also better. Figure 3: Chloride removal effi …
A novel process to recover sulfur in aqueous phase …
Huahong Shi & Tiancun Xiao. 4118 Accesses. 1 Citation. Explore all metrics. Abstract. Sulfur recovery is an important industrial process for fossil fuel clean …
PROCESS FOR THE RECOVERY AND FOR THE SEPARATION OF PURE SODIUM SULFATE
Finely ground Na 2 SO 4 seed crystals are introduced to an aqueous solution which is concentrated at a temperature greater than 60° C. to produce a first fraction consisting of ammonium sulfate with a minor amount of sodium sulfate, and a second fraction consisting of a predominant amount of sodium sulfate with a minor amount of …
Circulation of Sodium Sulfate Solution …
Hydrometallurgical recovery of rare earth elements (REE) from NiMH battery waste can be performed using sulfuric acid leaching followed by selective precipitation as double salt (REENa(SO4)2·H2O) …
Recovery of cobalt sulfate from spent lithium ion batteries …
The aim of this study was to focus on the leaching and separation of cobalt from other impurity metals in spent LIBs to recover pure cobalt sulfate for pigment use. 2. Materials and methods2.1. MaterialsThe spent LIBs were subjected to physical treatment which involved discharging, dehydration, drying and crushing steps (Shin et al., 2008).
Sustainable and efficient recovery of lithium from sodium sulfate …
Semantic Scholar extracted view of "Sustainable and efficient recovery of lithium from sodium sulfate by-product of lithium hydroxide production process using solvent extraction" by Licheng Zhang et al. ... An innovative scheme for the separation of potassium from lithium-bearing solution: A jarosite precipitation method ...
Process analysis and study of factors affecting the lithium …
Results indicate that mixing the lithium sulfate and sodium carbonate solutions both at 2.0 mol/L concentration at 45 °C and 300 rpm agitation rate followed by cooling crystallization of sodium sulfate byproduct produces lithium carbonate with 90% lithium recovery and 99.0% purity. With additional dissolution and recrystallization steps, …
Separation of sodium sulfate from high-salt …
In this paper, a material-oriented metallurgical electrolysis strategy, which is of such characteristics as short process, easy procedure, and nonpollution, is …
Separation of sodium sulfate from high-salt wastewater of …
The solubility data of sodium sulfate in the water-salt system of high-salt wastewater from lead-acid batteries are fitted, and the fitting formula is obtained as follows: X = − 10.7601 − 0.0947 T − 2.7592 × 10 − 4 T 2 + 2.6709 × 10 − 7 T 3. To ensure a high purity of sodium sulfate (98%), the concentration ratio of the sample ...
Sodium Sulphate Recovery from Industrial …
This paper review the efforts made for separation of Sodium sulphate from aqueous streams using membrane processes and applicability of nanofiltration membrane for …
General Principles and Strategies for Salting-Out Informed …
Overarching principles for salting-out extraction are long-established but poorly disseminated. We highlight the opportunity for more widespread application of this technique using the Hofmeister series as a foundational basis for choosing the right salt. The power of this approach is exemplified by the aqueous workup of a highly water …
Study on the recovery of purified MgSO 4·7H 2O crystals
The study reported 97% recovery of pure water from the liquid waste along with high purity calcium sulphate and sodium sulphate (with purities 98.0 and 96.4% respectively).
Solvent Extraction for Separation of 99.9% Pure Cobalt and Recovery …
In this work, hydrometallurgical recycling of metals from high-cobalt-content spent lithium-ion batteries (LIBs) from laptops was studied using precipitation and solvent extraction as alternative purification processes. Large amounts of cobalt (58% by weight), along with nickel (6.2%), manganese (3.06%) and lithium (6.09%) are present in LiCoO2 …
Process analysis and study of factors affecting the lithium …
Results indicate that mixing the lithium sulfate and sodium carbonate solutions both at 2.0 mol/L concentration at 45 °C and 300 rpm agitation rate followed by cooling crystallization of sodium sulfate byproduct produces lithium carbonate with 90% lithium recovery and 99.0% purity.
(PDF) Development of process flow sheet for recovery of high pure …
(1) Quantitative extraction of 99.99% pure cobalt sulfate can be obtained from LIBs industry waste using Cyanex 272 as an extractant by solvent extraction process from the leach liquor, by managing different process parameter such as pH of the leach liquor, Cyanex 272 concentration, O/A volume 368 B. Swain et al. / Separation and Purification ...
Electrolytic Salt Splitting for Sulfuric Acid and Caustic …
The Electrosynthesis Company and Ormiston Mining and Smelting Co. developed a process to split sodium sulfate, improving the current efficiency by …
The role of sodium-based additives on reduction process of …
1757-899X/478/1/012001. Abstract. In this present work, the selective reduction of nickel laterite was conducted by using 5 to 15 wt. % of sodium carbonate, sodium chloride and sodium sulfate as additives. The 5% wt. of palm shell charcoal was used as the reductant. The selective reduction process for nickel laterite was carried out at 1150°C ...
1.16: Methods for Separating Mixtures
Evaporation. Evaporation is a technique used to separate out homogeneous mixtures that contain one or more dissolved salts. The method drives off the liquid components from the solid components. The process typically involves heating the mixture until no more liquid remains. Prior to using this method, the mixture should only contain …
An efficiency strategy for cobalt recovery from simulated
de Araujo Sampaio, D. et al. Aqueous two-phase (polyethylene glycol+ sodium sulfate) system for caffeine extraction: Equilibrium diagrams and partitioning study. J. Chem. Thermodyn. 98, 86–94 ...
Process Flowsheet Development for Separation of Sm, Co, …
The precipitated double sulfate was later converted to Sm-oxalate, which was subsequently calcined to produce pure Sm 2 O 3. Following Sm separation, Fe was removed through precipitation by raising the pH to 3.0. For Cu and Co recovery, solvent extraction techniques using LIX 84I and Na-CYANEX 272, respectively, were followed.
Separation of sodium sulfate from high-salt …
At present, the idea of the common treatment process of zero-emission of industrial high-salt wastewater is to make the salt and water separate and recover the …
PROCESS FOR THE RECOVERY AND FOR THE …
Finely ground Na 2 SO 4 seed crystals are introduced to an aqueous solution which is concentrated at a temperature greater than 60° C. to produce a first fraction consisting of ammonium sulfate with a minor amount of sodium sulfate, and a second fraction …
All-Metal Recovery from Spent Ni-MH Batteries Based on
The experimental results of the separation of sulfuric acid from sodium sulfate by the membrane electrolysis method have been presented. The anion-exchange membrane Neosepta ACM has been used.
Co-production of potassium sulfate and sodium sulfate
What is claimed is: 1. A process for producing potassium sulfate or potassium sulfate and sodium sulfate from potash and a sodium sulfate/water source, comprising the steps of: (a) subjecting a sodium sulfate source to conversion with potash in an aqueous medium to yield glaserite precipitate and a first mother liquor;
4.8: Acid-Base Extraction
An acid-base extraction can be used to extract carboxylic acids from the organic layer into the aqueous layer. As was discussed in the previous section, NaOH can be used to convert a carboxylic acid into its more water-soluble ionic carboxylate form. However, if the mixture contains a desired compound that can react with NaOH, a milder base ...
Recovery of cobalt sulfate from spent lithium ion batteries …
However, some operations have inherent problems such as slow kinetics, solid–liquid separation, high cost, and low purity (Swain et al., 2004). Solvent extraction has been widely used for the recovery and separation of metals from leach liquors, effluents, and waste materials.